Setting up an experiment First, make sure that the DSC, RCS, and laptop are properly set up to run an experiment If the DSC computer is logged off, log on using the user name dsc and the password dscq Then, using tweezers, place your sample in the pan and record the mass. The appropriate mass range for samples is 1 mg to 10 mg. Be sure to specify a name and location for the data to be kept note that this text box is gray and can easily be missed. Discuss driver problems and ask for help from our community on our Free Driver Help Forum.
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Experiments can be set up using either the Experimental Wizard, or manually. If the run has a checkmark next to it and the sq905c dsc reads Completedsimply click the checkmark sq905c dsc reset the run. Windows 10, Windows 8. Once you are comfortable with the DSC methods and parameter settings, you can forgo the Wizard and set up the run yourself in the Experimental view.
For new users and even experienced sq905c dsc doing simple experimentsthe Wizard is usually best. Running an experiment From this point on, you will be controlling the experiment through the laptop. MSE Cornell more sq905c dsc.
Creating samples If you are starting with a bulk piece of material, it is necessary to convert this to a form that can be used in the DSC.
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Sq905c dsc Camera Supported OS: Or you can request a driver and we will find it for you. For specific information on these functions and general help in using Universal Analysis, consult the UA Manual or Getting Started Guide, both located in the “Senior Ss905c folder on the desktop. If a language option is given, select your language. Sometimes at this point, you will sq905c dsc an error message sq905cc says the sq9055c acceptor is not responding.
For most experiments, non-hermetic pans ones that don’t seal airtight are appropriate, although sq905c dsc experiments may call for hermetic or high-volume pans. There are three views to choose from, and they are selected under the View sq905c dsc. Sample pans and lids are in the wooden “TA” box. Sq905c dsc 98Win 95 File Size: From this point on, you will be controlling the experiment sq905c dsc the laptop. Before performing any experiments or calibrations, all DSC users sq905c dsc view the document, which includes safety precautions and basic operating principles and instructions for the DSC and Refrigerated Cooling System RCS.
The three tabs SummaryProcedureand Notes each allow you to enter the parameters as zq905c would in the Wizard. Disconnect the device from your computer. File extensions are of the form. The run you wish to start should have the arrow pointing to it and a dot sq905c dsc to ddsc.
No matter what, you should dsd touch a sample with your bare hands. The reference pan will usually be in place already, and can be left in place when you finish. Check the Sequence run list on the left side of the screen. Digital Camera File Version: If this occurs, simply restart the computer.
Once both pans are in place, close the lid. Weighing and encapsulating samples Once you have a small sq950c, it sq905c dsc important to accurately measure its mass because this sq905c dsc entered into the DSC so that it can give you data that sq905c dsc independent of sample size. Open the lid, use dsf tweezers for the internal lid.
Place them in the sample press, sq905c dsc place the lid on top also open-side-up as shown in Figure 3. Once you have a small piece, it is important to accurately measure its mass because this is qs905c into the DSC so that it can give you data that is independent of sample size. This indicates ss905c the run is selected and ready to go. Reconnect the device and power it on. Metal samples should be roughly the size shown in Figure 2. Using the metal tweezers there should be a pair on or next to the DSCplace the sample and reference pans on the sq905c dsc as shown in Figure sq905c dsc, centering both as well as possible.
Experimental view shows your experiment parameters and allows you to edit them. One of the advantages of the Wizard is that it handles all of this for you.
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How to Install Drivers After you have found the right device driver, follow these sq90c instructions to install it. Once you begin the experiment, it is okay to leave the DSC, but it sq905c dsc recommended that you wait until the run has reached its initial temperature sq905c dsc begun collecting data.
Eq905c are likely to have zq905c surface oxide, in which case you will want to sq905f this off of a small area and start with a clean surface.
Once the DSC is ready to go, you can put your sample into the cell. Once you are ready to begin the experiment: When you go back into the software, it should have maintained your settings. After the experiment begins, it will display to the left of where it said Standby and now says Running the approximate time left in the experiment. Browse the list below sq905c dsc find sq905c dsc driver that meets your needs. If you do not specify a name, sa905c will collect data with a name that is incremented from the previous experiment, so you sq905c dsc not be able to find your data file if you lose track of this.
If the bulk material is too hard to cut a big enough sample with a razor blade, you may need to be patient and cut and collect small shavings. Selecting this allows you to run more complex experiments that combine the various heating, cooling, and isothermal processes as you wish. Prepared reference pans are normally already in the DSC cell; if not they can be found in the vial labeled “MT”, or you can simply make your own.
If you wish to analyze sq905c dsc on another computer, the analysis software is available to be installed for free, or the sq905c dsc can be exported into a delimited plain text format. Win ME File Size: Discuss driver problems and ask for help from our community on ssc Free Driver Help Forum.